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2 article(s) from Lincoln, Stephen F

β-Cyclodextrin- and adamantyl-substituted poly(acrylate) self-assembling aqueous networks designed for controlled complexation and release of small molecules

Liang Yan,
Duc-Truc Pham,
Philip Clements,
Stephen F. Lincoln,
Jie Wang,
Xuhong Guo and
Christopher J. Easton

Beilstein J. Org. Chem. 2017, 13, 1879–1892, doi:10.3762/bjoc.13.183

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Graphical Abstract

Figure 1: β-Cyclodextrin- and adamantyl-substituted poly(acrylate)s PAAβ-CDen, PAAADen, PAAADhn, and PAAADddn...

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Figure 2: ITC data for the PAAβ-CDen/PAAADen, system obtained in aqueous Na₂HPO₄/KH₂PO₄ pH 7.0 buffer at I = ...

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Figure 3: ITC data for the PAAβ-CDen/PAAADddn system obtained in aqueous Na₂HPO₄/KH₂PO₄ pH 7.0 buffer at I = ...

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Figure 4: Representation of ditopic complexation of an ADddn substituent of PAAADddn, by two β-CDen substitue...

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Figure 5: 2D NOESY ¹H NMR spectrum of 0.44 wt % PAAβ-CDen ([β-CDen] = 2.0 × 10⁻³ mol dm⁻³) and 0.60 wt % PAAA...

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Figure 6: (a) Molar absorbance variation of 1.5 cm³ of a EO solution ([EO] = 2.00 × 10⁻⁵ mol dm⁻³) with 20 se...

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Figure 7: (a) Molar absorbance variation of 1.5 cm³ of a EO solution ([EO] = 2.00 × 10⁻⁵ mol dm⁻³) with 20 se...

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Figure 8: Speciation plot with [β-CDen]_total = 100% for the PAAβ-CDen/PAAADhn/EO system.

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Figure 9: 2D NOESY ¹H NMR spectrum of MR ([MR] = 2.0 × 10⁻³ mol dm⁻³) in solution with PAAβ-CDen (0.78 wt %, ...

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Figure 10: Viscosity variations at a 0.03 s⁻¹ shear rate of 1.14 wt % PAAβ-CDen/PAAADen, 1.18 wt % PAAβ-CDen/P...

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Figure 11: Representation of dye complexation in the PAAβ-CDen/PAAADen and PAAβ-CDen/PAAADhn networks.

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Figure 12: Release profiles for EO (i), MO (ii) and MR (iii) from aqueous (a) Na₂HPO₄/KH₂PO₄ buffer alone, (b)...

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Full Research Paper

Published 07 Sep 2017

Full text

Supramolecular polymer assembly in aqueous solution arising from cyclodextrin host–guest complexation

Jie Wang,
Zhiqiang Qiu,
Yiming Wang,
Li Li,
Xuhong Guo,
Duc-Truc Pham,
Stephen F. Lincoln and
Robert K. Prud’homme

Beilstein J. Org. Chem. 2016, 12, 50–72, doi:10.3762/bjoc.12.7

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Graphical Abstract

Figure 1: Structures of α-, β- and γ-CD. Individual carbon atom numbering is shown for one D-glucopyranose su...

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Figure 2: Associations of hydrophobic substituents (circled) (a) and their disruption through host–guest comp...

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Figure 3: Decrease of aqueous solution viscosity at a shear rate of 50 s⁻¹ due to α-CD (circles), β-CD (recta...

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Figure 4: The effect of (a) α-CD, (b) β-CD and (c) γ-CD on the hydrophobic interactions between n-C₁₈H₃₇ subs...

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Figure 5: The effect of SDS addition on viscosity shear rate dependence for 2 wt % aqueous PAAodn solutions c...

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Figure 6: Host–guest complexation between polymers with cyclodextrin and hydrophobic substituents.

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Figure 7: Variation of viscosity with mole ratio of CD substituents to hydrophobic substituents on poly(acryl...

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Figure 8: Illustration of the competitive intermolecular host–guest complexation of either the adamantyl subs...

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Figure 9: Competitive host–guest complexations in which either the adamantyl substituent (red) or the n-hexyl...

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Figure 10: (a) Substituted chitosan in which acyl- and adamantyl-substitution is 5% and 12 %, respectively. (b...

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Figure 11: The formation of a AD-PEG micelle followed by the formation of a AD-PEG/α-CD supramolecular hydroge...

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Figure 12: Interaction of PEG-b-PAA block copolymer with cis-diamminedichloroplatinum(II), cisplatin, to form ...

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Figure 13: Solution to hydrogel transitions (a)–(d) for a PAAddn segment in the presence of competitive photo-...

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Figure 14: Structures of the poly(acrylate)-based polymers PAAAzo (trans), PAAAzo (cis), PAA3α-CD and PAA6α-CD...

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Figure 15: Variation of viscosity of a PAA6α-CD/PAAAzo solution (circles) and a PAA3α-CD/PAAAzo solution (tria...

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Figure 16: The structures proposed for the poly(ethylene glycol)-b-poly(ethylamine)-g-dextran·γ-CD, PEG-PEI-de...

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Figure 17: Structure of poly(ethylene glycol) polyrotaxane with adamantyl end substituents, and its temperatur...

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Figure 18: Copolymers of either (a) N,N-dimethylacrylamide (DMAA) or (b) N-isopropylacrylamine (NIPAAM) with 1...

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Figure 19: The copolymer of isopropylacrylamine and methacrylated β-CD (a) and its complexation of the anions ...

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Figure 20: Solution to hydrogel transitions for two segments of PAAddn in the presence of β-CD and change in t...

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Figure 21: Preparation of a β-CD and adamantyl substituted acrylamide polymer hydrogel involving host–guest co...

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Figure 22: Aqueous solutions of the polymers poly-β-CD and poly-α-BrNP form the poly-β-CD/poly-α-BrNP hydrogel ...

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Figure 23: (a) Randomly β-CD substituted poly(acrylate), PAA-6β-CD. (b) Randomly ferrocenyl substituted poly(a...

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Figure 24: (a) The β-CD, adamantyl and ferrocenyl substituted pAAm and pNiPAAM polymers. (b) The β-CD, adamant...

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Review

Published 12 Jan 2016

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